4XH0
Structure of C. glabrata Hrr25 bound to ADP (SO4 condition)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-10-15 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 71.788, 76.974, 84.277 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.499 - 1.990 |
R-factor | 0.1676 |
Rwork | 0.166 |
R-free | 0.20040 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.250 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.800 | 2.100 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.095 | 0.910 |
Number of reflections | 31839 | |
<I/σ(I)> | 11.9 | 2.4 |
Completeness [%] | 98.0 | 98.6 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M Bis-Tris pH 6.5, 0.2 M lithium sulfate, 19% PEG 3350, and 5 mM TCEP |