4XGR

Crystal structure of addiction module from Mycobacterial species

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-06-22
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97912
Spacegroup name	P 31 2 1
Unit cell lengths	96.310, 96.310, 233.033
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	48.150 - 2.700
R-factor	0.24444
Rwork	0.243
R-free	0.27757
RMSD bond length	0.010
RMSD bond angle	1.421
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	48.150
High resolution limit [Å]	2.700
Number of reflections	34963
<I/σ(I)>	37.037
Completeness [%]	98.9
Redundancy	6.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M sodium acetate, 0.1 M sodium citrate at pH 5.5, and 5% (w/v) PEG4000