4XGQ
Crystal structure of addiction module from Mycobacterial species
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-09-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 96.381, 96.381, 232.788 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.660 - 2.700 |
R-factor | 0.20736 |
Rwork | 0.206 |
R-free | 0.23814 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.212 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.660 |
High resolution limit [Å] | 2.700 |
Number of reflections | 35181 |
<I/σ(I)> | 40.96 |
Completeness [%] | 99.3 |
Redundancy | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M sodium citrate tribasic dihydrate pH 5.6, 1.0M ammonium phosphate monobasic |