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4XCK

Vibrio cholerae O395 Ribokinase complexed with ADP, Ribose and Cesium ion.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsCu FINE FOCUS
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2014-12-02
DetectorMAR scanner 345 mm plate
Wavelength(s)1.54
Spacegroup nameP 1
Unit cell lengths59.304, 69.553, 78.316
Unit cell angles106.99, 98.77, 96.46
Refinement procedure
Resolution26.643 - 2.370
R-factor0.1914
Rwork0.188
R-free0.25070
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1rk2
RMSD bond length0.013
RMSD bond angle1.278
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.8_1069))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.410
High resolution limit [Å]2.3702.370
Rmerge0.070
Number of reflections47045
<I/σ(I)>5.11.5
Completeness [%]93.893.4
Redundancy2.12.11
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6293PEG 6000, 0.1M MES BUFFER, pH 6.0

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