4XAV
Crystal structure of olfactomedin domain from gliomedin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 80 |
| Detector technology | CCD |
| Collection date | 2014-11-06 |
| Detector | RAYONIX MX300HS |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.164, 140.643, 78.152 |
| Unit cell angles | 90.00, 106.03, 90.00 |
Refinement procedure
| Resolution | 44.646 - 2.052 |
| R-factor | 0.1678 |
| Rwork | 0.166 |
| R-free | 0.21370 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.924 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.650 |
| High resolution limit [Å] | 2.050 |
| Number of reflections | 59953 |
| <I/σ(I)> | 9.05 |
| Completeness [%] | 98.2 |
| Redundancy | 5.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | phosphate citrate pH 5.5 PEG 600 |
