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4XA9

Crystal structure of the complex between the N-terminal domain of RavJ and LegL1 from Legionella pneumophila str. Philadelphia

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2014-11-07
DetectorADSC QUANTUM 315r
Wavelength(s)0.97924
Spacegroup nameC 1 2 1
Unit cell lengths219.608, 120.885, 149.288
Unit cell angles90.00, 92.05, 90.00
Refinement procedure
Resolution29.943 - 2.000
R-factor0.1595
Rwork0.158
R-free0.19460
Structure solution methodSAD
RMSD bond length0.006
RMSD bond angle0.854
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareSHELX
Refinement softwarePHENIX ((phenix.refine: 1.9_1692))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.030
High resolution limit [Å]2.0002.000
Rmerge0.0430.208
Number of reflections258259
<I/σ(I)>21.144.82
Completeness [%]97.894.4
Redundancy3.52.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.52980.1 M NaCl, 100 mM Tris pH 8.5 and 26% (w/v) PEG3350

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