4X2M

Structure of Mtr2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Collection date	2011-11-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9686
Spacegroup name	P 41 21 2
Unit cell lengths	83.958, 83.958, 131.340
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.819 - 2.000
R-factor	0.1818
Rwork	0.181
R-free	0.20180
RMSD bond length	0.003
RMSD bond angle	0.716
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	38.827
High resolution limit [Å]	2.000
Number of reflections	31939
<I/σ(I)>	12.2
Completeness [%]	98.7
Redundancy	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	1.26 M Ammonium Sulphate, 0.1 M MES pH 6.0. See publication for details.