4X1Z
Crystal structure of RHDVb P domain in complex with H type 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-05 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.984463 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.170, 76.210, 107.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.997 - 1.360 |
R-factor | 0.109 |
Rwork | 0.108 |
R-free | 0.13240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4x1w |
RMSD bond length | 0.007 |
RMSD bond angle | 1.246 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.330 | |
High resolution limit [Å] | 1.300 | 5.810 | 1.300 |
Rmerge | 0.066 | 0.041 | 0.454 |
Rmeas | 0.068 | 0.043 | 0.540 |
Total number of observations | 2048689 | ||
Number of reflections | 151500 | 1870 | 9777 |
<I/σ(I)> | 22.18 | 51.55 | 1.89 |
Completeness [%] | 98.3 | 96.6 | 86.3 |
Redundancy | 13.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 291 | Lithium chloride, PEG 6000, Citric Acid |