4X0W
The crystal structure of mupain-1-17 in complex with murinised human uPA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-11-24 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.979 |
| Spacegroup name | H 3 |
| Unit cell lengths | 120.641, 120.641, 42.657 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 60.320 - 2.100 |
| R-factor | 0.23788 |
| Rwork | 0.236 |
| R-free | 0.27222 |
| RMSD bond length | 0.048 |
| RMSD bond angle | 2.807 |
| Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 99.000 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 12802 |
| <I/σ(I)> | 14.8 |
| Completeness [%] | 94.6 |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | 2.0 M ammonium sulfate, 50 mM sodium citrate pH 4.6, 5% PEG 400 |
