4WZT
Crystal structure of P domain from norovirus strain NSW0514 in complex with HBGA type A (triglycan)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.978174 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 104.740, 104.740, 190.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.258 - 1.910 |
R-factor | 0.1549 |
Rwork | 0.154 |
R-free | 0.17910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4oos |
RMSD bond length | 0.008 |
RMSD bond angle | 1.134 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.3) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.260 | 1.900 | |
High resolution limit [Å] | 1.850 | 8.280 | 1.850 |
Rmerge | 0.087 | 0.019 | 0.983 |
Rmeas | 0.094 | 0.021 | 1.063 |
Total number of observations | 585432 | ||
Number of reflections | 89901 | 1063 | 6523 |
<I/σ(I)> | 16.68 | 59.5 | 1.6 |
Completeness [%] | 98.8 | 88.1 | 98.3 |
Redundancy | 6.5 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG 3350, Sodium formate |