4WYT
Crystal Structure of Scribble PDZ34 tandem at 2.6 Angstroms
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-11 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9792 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 69.140, 70.850, 92.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.658 - 2.600 |
R-factor | 0.2283 |
Rwork | 0.226 |
R-free | 0.28300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1tp3 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.521 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.483 | 46.375 | 2.740 |
High resolution limit [Å] | 2.600 | 8.220 | 2.600 |
Rmerge | 0.041 | 0.575 | |
Rmeas | 0.136 | ||
Rpim | 0.055 | 0.020 | 0.255 |
Total number of observations | 44038 | 1323 | 6451 |
Number of reflections | 7301 | ||
<I/σ(I)> | 10.2 | 15.4 | 3.9 |
Completeness [%] | 100.0 | 99 | 100 |
Redundancy | 6 | 5 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 3.0 M sodium chloride, 0.1M Tris-Hcl |