4WXW
SadC (323-487) from Pseudomonas aeruginosa PAO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-09-20 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.913, 51.102, 54.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.295 - 1.800 |
R-factor | 0.1863 |
Rwork | 0.185 |
R-free | 0.21700 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.097 |
Data reduction software | SCALEPACK |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.800 |
Number of reflections | 13694 |
<I/σ(I)> | 36.2 |
Completeness [%] | 99.1 |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293.15 | 0.1 M Tris-HCl, 0.2 M MgCl, 26% PEG3350, 25 mM nonanoyl-N-methylglucamide |