4WXA
Crystal structure of binary complex Gon7-Pcc1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 2 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-05-24 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9801 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 80.730, 104.390, 89.890 |
| Unit cell angles | 90.00, 111.55, 90.00 |
Refinement procedure
| Resolution | 44.280 - 2.440 |
| R-factor | 0.22677 |
| Rwork | 0.225 |
| R-free | 0.26991 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.711 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0071) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.280 | 2.530 |
| High resolution limit [Å] | 2.440 | 2.443 |
| Number of reflections | 25516 | |
| <I/σ(I)> | 14.69 | |
| Completeness [%] | 99.1 | 94.59 |
| Redundancy | 3.69 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M Sodium Acetate pH 6.5, 20% PEG1500, 20% Glycerol, 3% Methanol |
