4WWR
Crystal Structure of Bag6-Ubl4A Dimerization Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-10-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.235, 56.494, 75.545 |
Unit cell angles | 90.00, 96.23, 90.00 |
Refinement procedure
Resolution | 19.647 - 2.000 |
R-factor | 0.2267 |
Rwork | 0.225 |
R-free | 0.26880 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.072 |
Data scaling software | Aimless (0.3.6) |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.650 | 19.650 | 2.050 |
High resolution limit [Å] | 2.000 | 8.940 | 2.000 |
Rmerge | 0.047 | 0.013 | 0.813 |
Rpim | 0.033 | 0.010 | 0.565 |
Total number of observations | 78055 | 818 | 5819 |
Number of reflections | 26499 | ||
<I/σ(I)> | 13.9 | 49.6 | 1.7 |
Completeness [%] | 98.6 | 88.7 | 98.2 |
Redundancy | 2.9 | 2.8 | 3 |
CC(1/2) | 0.999 | 0.999 | 0.620 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298.13 | 20% PEG-3350, 0.05 HEPES sodium pH 7.0, 1% tryptone |