4WVY
Double-heterohexameric rings of full-length Rvb1(ATP)/Rvb2(apo)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-07-23 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.91889 |
Spacegroup name | H 3 2 |
Unit cell lengths | 210.348, 210.348, 137.140 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.690 - 3.640 |
R-factor | 0.2229 |
Rwork | 0.221 |
R-free | 0.25060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2c9o |
RMSD bond length | 0.008 |
RMSD bond angle | 1.000 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.21) |
Phasing software | PHASER |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 109.748 | 33.694 | 3.840 |
High resolution limit [Å] | 3.640 | 11.510 | 3.640 |
Rmerge | 0.073 | ||
Rmeas | 0.133 | ||
Rpim | 0.035 | 0.021 | 0.287 |
Total number of observations | 190173 | 5701 | 26988 |
Number of reflections | 13158 | ||
<I/σ(I)> | 15.9 | 32.7 | 3.9 |
Completeness [%] | 99.9 | 96 | 100 |
Redundancy | 14.5 | 13.3 | 14.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 1 M sodium malonate pH 6.0 |