4WU9

Structure of cisPtNAP-NCP145

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	98.15
Detector technology	CCD
Collection date	2011-07-01
Detector	MAR CCD 165 mm
Wavelength(s)	1.07
Spacegroup name	P 21 21 21
Unit cell lengths	106.570, 109.330, 181.280
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	70.330 - 2.600
R-factor	0.218
Rwork	0.216
R-free	0.27300
RMSD bond length	0.007
RMSD bond angle	1.407
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	70.330
High resolution limit [Å]	2.600
Number of reflections	58392
Completeness [%]	89.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	291.15	Manganese chloride, potassium chloride, potassium cacodylate