4WSV
The crystal structure of hemagglutinin from A/Taiwan/1/2013 in complex with 6'SLN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-03-22 |
| Detector | MARMOSAIC 325 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 186.438, 99.584, 134.216 |
| Unit cell angles | 90.00, 125.96, 90.00 |
Refinement procedure
| Resolution | 49.772 - 3.100 |
| R-factor | 0.2478 |
| Rwork | 0.246 |
| R-free | 0.27900 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.272 |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 3.000 |
| Number of reflections | 37065 |
| <I/σ(I)> | 13.1 |
| Completeness [%] | 94.8 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 8.5 | 293 | 0.01M nickel chloride, 0.1 M Tris-HCl pH 8.5 and 20% (w/v) PEG 2000MME |
