4WSS
The crystal structure of hemagglutinin form A/chicken/New York/14677-13/1998 in complex with LSTa
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-BM |
| Synchrotron site | APS |
| Beamline | 22-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-03-20 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 254.967, 134.779, 122.622 |
| Unit cell angles | 90.00, 112.20, 90.00 |
Refinement procedure
| Resolution | 45.200 - 2.800 |
| R-factor | 0.22128 |
| Rwork | 0.220 |
| R-free | 0.25402 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.584 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.200 |
| High resolution limit [Å] | 2.800 |
| Number of reflections | 92840 |
| <I/σ(I)> | 17 |
| Completeness [%] | 98.5 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 293 | 0.2 M ammonium fluoride and 20% (w/v) PEG 3350 |
