4WSR
The crystal structure of hemagglutinin form A/chicken/New York/14677-13/1998
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-20 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 252.545, 134.822, 123.093 |
Unit cell angles | 90.00, 113.23, 90.00 |
Refinement procedure
Resolution | 48.000 - 2.500 |
R-factor | 0.21176 |
Rwork | 0.210 |
R-free | 0.24617 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.601 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.000 |
High resolution limit [Å] | 2.500 |
Number of reflections | 129493 |
<I/σ(I)> | 30.6 |
Completeness [%] | 99.0 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 293 | 0.2 M ammonium fluoride, 20% (w/v) PEG 3350 |