4WSI
Crystal Structure of PALS1/Crb complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 111.928, 111.928, 223.065 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.523 - 2.950 |
R-factor | 0.2084 |
Rwork | 0.207 |
R-free | 0.23500 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.684 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.000 |
High resolution limit [Å] | 2.950 | 8.000 | 2.950 |
Rmerge | 0.083 | 0.048 | 0.761 |
Total number of observations | 359841 | ||
Number of reflections | 30528 | ||
<I/σ(I)> | 12.1 | ||
Completeness [%] | 99.6 | 93.1 | 100 |
Redundancy | 11.8 | 9.4 | 12.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 5% PEG3350, 5-10% Tacsimate pH 6.0 |