4WPX
Chaetomium theromophilum TREX2 CID domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-30 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9700 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.528, 168.288, 69.223 |
Unit cell angles | 90.00, 112.21, 90.00 |
Refinement procedure
Resolution | 19.904 - 3.310 |
R-factor | 0.2207 |
Rwork | 0.218 |
R-free | 0.27660 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.792 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.904 |
High resolution limit [Å] | 3.310 |
Number of reflections | 17487 |
<I/σ(I)> | 6.9 |
Completeness [%] | 98.0 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | see publication for details |