4WPM

Structure of the Chaetomium thermophilum Mex67:Mtr2 Complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-01-31
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9686
Spacegroup name	C 1 2 1
Unit cell lengths	113.731, 29.796, 52.453
Unit cell angles	90.00, 96.53, 90.00

Refinement procedure

Resolution	40.679 - 2.400
R-factor	0.2294
Rwork	0.229
R-free	0.24640
RMSD bond length	0.002
RMSD bond angle	0.677
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	40.700
High resolution limit [Å]	2.400
Number of reflections	7066
<I/σ(I)>	5.7
Completeness [%]	99.6
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	see publication for details