4WP6
Structure of the Mex67 LRR domain from Chaetomium thermophilum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 113.817, 33.100, 43.495 |
Unit cell angles | 90.00, 91.65, 90.00 |
Refinement procedure
Resolution | 43.477 - 1.700 |
R-factor | 0.1873 |
Rwork | 0.185 |
R-free | 0.21330 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.021 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.500 |
High resolution limit [Å] | 1.700 |
Number of reflections | 18096 |
<I/σ(I)> | 9.5 |
Completeness [%] | 99.8 |
Redundancy | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | see publication for details |