4WP2
Chaetomium Mex67 UBA domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-03-30 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9200 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 95.903, 95.903, 74.967 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 41.527 - 1.700 |
| R-factor | 0.2003 |
| Rwork | 0.198 |
| R-free | 0.24020 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.051 |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 48.000 |
| High resolution limit [Å] | 1.700 |
| Number of reflections | 44143 |
| <I/σ(I)> | 19.8 |
| Completeness [%] | 100.0 |
| Redundancy | 16.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | see publication for precise details. Cacodylate buffer employed. |
