Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4WOU

Crystal Structure of Mtb PEPCK in complex with GDP and metals

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-B
Synchrotron siteAPS
Beamline23-ID-B
Temperature [K]120
Detector technologyCCD
Collection date2011-04-07
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)0.91993
Spacegroup nameC 2 2 21
Unit cell lengths103.316, 125.172, 122.147
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution47.578 - 2.122
R-factor0.179
Rwork0.177
R-free0.21120
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.105
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareMOLREP
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.122
Rmerge0.110
Number of reflections44852
<I/σ(I)>27.75
Completeness [%]99.8
Redundancy8.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP28910% (w/v) PEG 3350, 0.2 M KH2PO4

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon