4WOA

Lysozyme Multiple Crystals After Surface Acoustic Wave Alignment

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X25
Synchrotron site	NSLS
Beamline	X25
Temperature [K]	100
Detector technology	CCD
Collection date	2014-07-10
Detector	ADSC QUANTUM 315
Wavelength(s)	1.10
Spacegroup name	P 43 21 2
Unit cell lengths	77.895, 77.895, 37.498
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.948 - 1.800
R-factor	0.1956
Rwork	0.192
R-free	0.22800
RMSD bond length	0.006
RMSD bond angle	1.019
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.800
Number of reflections	58646
<I/σ(I)>	21.2
Completeness [%]	98.0
Redundancy	5.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE	4.6	277	1 M NaCl, 0.1 M Na Acetate, 25% Glycerol, gentle agitation