4WO6
Lysozyme Pre-surface acoustic wave
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-03-30 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.978 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.349, 79.349, 37.597 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.054 - 2.001 |
R-factor | 0.1592 |
Rwork | 0.154 |
R-free | 0.20920 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.034 |
Data reduction software | HKL-2000 |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 64483 |
<I/σ(I)> | 16.8 |
Completeness [%] | 100.0 |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 4.6 | 277 | 1 M NaCl, 25% Glycerol, 0.1 M Na Acetate, pH 4.6, gentle agitation |