4WKZ
Complex of autonomous ScaG cohesin CohG and X-doc domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-16 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | .97250 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 74.029, 211.781, 36.666 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 105.890 - 1.790 |
R-factor | 0.18075 |
Rwork | 0.179 |
R-free | 0.22273 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.525 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.820 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.180 | 0.333 |
Number of reflections | 56262 | |
<I/σ(I)> | 8.1 | 1.85 |
Completeness [%] | 87.2 | |
Redundancy | 4.2 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | No 37 of Crystal Screen kit from Hampton Research |