4WJS
Crystal structure of Rsa4 from Chaetomium thermophilum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-03 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 48.155, 48.832, 58.625 |
Unit cell angles | 67.47, 88.39, 62.65 |
Refinement procedure
Resolution | 42.070 - 1.800 |
R-factor | 0.1676 |
Rwork | 0.165 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1nex |
RMSD bond length | 0.007 |
RMSD bond angle | 1.014 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.070 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.044 | 0.284 |
Number of reflections | 37846 | |
<I/σ(I)> | 6.7 | 2.5 |
Completeness [%] | 94.7 | 93.3 |
Redundancy | 1.8 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2 mM KF, 20% PEG 3350 |