4WJA

Crystal Structure of PAXX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2014-04-22
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.979
Spacegroup name	P 65 2 2
Unit cell lengths	91.825, 91.825, 152.468
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	38.475 - 2.600
R-factor	0.2473
Rwork	0.245
R-free	0.26650
Structure solution method	SAD
RMSD bond length	0.012
RMSD bond angle	1.566
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	79.523
High resolution limit [Å]	2.600
Number of reflections	12287
<I/σ(I)>	69.64
Completeness [%]	99.3
Redundancy	20

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.5	289	2.24M Ammonium sulfate, 0.1M Bis-Tris, pH 5.5