4WIK
HUMAN SPLICING FACTOR, CONSTRUCT 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-10-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 127.399, 180.416, 57.029 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.200 - 3.000 |
R-factor | 0.244 |
Rwork | 0.242 |
R-free | 0.29100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.980 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.200 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.083 | 0.694 |
Number of reflections | 13401 | |
<I/σ(I)> | 8.7 | 1.9 |
Completeness [%] | 99.2 | 99.8 |
Redundancy | 4.1 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M SODIUM PHOSPHATE DIBASIC DIHYDRATE, 22% (W/V) POLYETHYLENE GLYCOL 3350, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 293K |