4WHD
Human CEACAM1 N-domain homodimer
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-08-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 4 21 2 |
| Unit cell lengths | 107.573, 107.573, 63.960 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 76.070 - 2.500 |
| R-factor | 0.1872 |
| Rwork | 0.183 |
| R-free | 0.22590 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.647 |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 76.070 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 13472 |
| <I/σ(I)> | 18.63 |
| Completeness [%] | 99.0 |
| Redundancy | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 295 | PEG 3000, NaCl, Phosphate-Citrate |
