4WHC
Human CEACAM6 N-domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-07-23 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | P 63 |
| Unit cell lengths | 91.912, 91.912, 60.359 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.100 - 2.705 |
| R-factor | 0.1922 |
| Rwork | 0.188 |
| R-free | 0.22660 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.459 |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.100 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 8009 |
| <I/σ(I)> | 35.9 |
| Completeness [%] | 99.4 |
| Redundancy | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 295 | 20% PEG 3000, 100 mM Imidazole pH 8.0, 200 mM ZnAc |
