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4WH3

N-acetylhexosamine 1-kinase in complex with ATP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]100
Detector technologyCCD
Collection date2014-01-26
DetectorADSC QUANTUM 315r
Wavelength(s)0.97924
Spacegroup nameP 21 21 21
Unit cell lengths44.030, 88.471, 105.219
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution32.604 - 1.800
R-factor0.1906
Rwork0.189
R-free0.22220
Structure solution methodSAD
RMSD bond length0.007
RMSD bond angle1.067
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.830
High resolution limit [Å]1.8001.800
Rmerge0.0460.408
Number of reflections73240
<I/σ(I)>43.44.6
Completeness [%]99.099.8
Redundancy7.57
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.5293PEG 8000, magnesium acetate, sodium cacodylate

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