4WGZ
Crystal Structure of Cytochrome c' from Alcaligenes xylosoxidans NCIMB 11015 at pH 6.0
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NE3A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-05-13 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 53.189, 53.189, 181.026 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 26.310 - 1.110 |
| R-factor | 0.14158 |
| Rwork | 0.141 |
| R-free | 0.16168 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1e83 |
| RMSD bond length | 0.030 |
| RMSD bond angle | 3.094 |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.100 |
| Number of reflections | 62734 |
| <I/σ(I)> | 36.1 |
| Completeness [%] | 99.4 |
| Redundancy | 11.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 6 | 293 | 12 % PEG4000, 100 mM potassium phosphate, 1 mM sodium azide |
