4WE8
The crystal structure of hemagglutinin of influenza virus A/Victoria/361/2011
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-03-16 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.0 |
Spacegroup name | H 3 2 |
Unit cell lengths | 100.911, 100.911, 383.361 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.156 - 2.100 |
R-factor | 0.1923 |
Rwork | 0.190 |
R-free | 0.22730 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.931 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.100 |
Number of reflections | 43789 |
<I/σ(I)> | 37.1 |
Completeness [%] | 98.5 |
Redundancy | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 10.5 | 293 | 0.1M CAPS:NaOH, 30% PEG 400 |