4WE2
Donor strand complemented FaeG of F4ab fimbriae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.639, 49.026, 54.468 |
Unit cell angles | 90.00, 109.21, 90.00 |
Refinement procedure
Resolution | 51.430 - 1.500 |
R-factor | 0.17704 |
Rwork | 0.175 |
R-free | 0.21396 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hlr |
RMSD bond length | 0.021 |
RMSD bond angle | 2.058 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.430 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 41977 | |
<I/σ(I)> | 13.8 | 2.8 |
Completeness [%] | 97.9 | 89.1 |
Redundancy | 3.1 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 18 mM Na/K-phosphate, 18% PEG 3350 |