4WBP

Crystal structure of the HR-1 domain of human caprin-1 in the P3121 space group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-F
Synchrotron site	APS
Beamline	21-ID-F
Temperature [K]	100
Detector technology	CCD
Collection date	2014-08-22
Detector	MAR CCD 165 mm
Wavelength(s)	0.97872
Spacegroup name	P 31 2 1
Unit cell lengths	66.000, 66.000, 117.701
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.230 - 2.500
R-factor	0.2177
Rwork	0.212
R-free	0.26560
RMSD bond length	0.004
RMSD bond angle	0.914
Refinement software	PHENIX ((phenix.refine: 1.8.2_1309))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.230	2.640
High resolution limit [Å]	2.500	2.500
Number of reflections	10750
<I/σ(I)>	12.3	2.3
Completeness [%]	100.0	100
Redundancy	9.6	9.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	298	12% PEG600, 0.1 M Tris, 0.1 M Calcium acetate, 10% glycerol