4WBF

Acinetobacter baumannii SDF NDK

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	180
Detector technology	CCD
Collection date	2014-09-01
Detector	RIGAKU SATURN 944
Wavelength(s)	1.5419
Spacegroup name	I 2 2 2
Unit cell lengths	60.330, 75.400, 82.120
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.107 - 2.640
R-factor	0.2068
Rwork	0.201
R-free	0.25810
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4w98
RMSD bond length	0.009
RMSD bond angle	1.102
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	47.110
High resolution limit [Å]	2.490
Number of reflections	6880
<I/σ(I)>	7.3
Completeness [%]	100.0
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	289	Sodium malonate, HEPES, Jeffamine ED-2001