4WAS
STRUCTURE OF THE ETR1P/NADP/CROTONYL-COA COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2013-11-22 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 147.920, 106.140, 94.410 |
Unit cell angles | 90.00, 98.41, 90.00 |
Refinement procedure
Resolution | 37.815 - 1.700 |
R-factor | 0.1882 |
Rwork | 0.188 |
R-free | 0.22420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1n9g |
RMSD bond length | 0.008 |
RMSD bond angle | 1.178 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.900 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 156706 | |
<I/σ(I)> | 10.6 | 1 |
Completeness [%] | 99.0 | 98.9 |
Redundancy | 3.1 | 3.03 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 292 | 2M ammonium sulfate, 0.1M ADA/NaOH pH 7 |