4WAA
Crystal structure of Nix LIR-fused human LC3B_2-119
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-21 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 67.385, 67.385, 116.875 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.150 - 2.350 |
R-factor | 0.20311 |
Rwork | 0.200 |
R-free | 0.27283 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vtu |
RMSD bond length | 0.013 |
RMSD bond angle | 1.558 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.990 | 2.480 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.157 | 0.567 |
Number of reflections | 11860 | |
<I/σ(I)> | 15.7 | 5.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4 | 300 | 20% PEG3350, 8% Tacsimate pH 4 |