4WA2
The crystal structure of hemagglutinin from a H3N8 influenza virus isolated from New England harbor seals in complex with 3'SLN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-01-11 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 |
| Unit cell lengths | 79.541, 102.327, 109.666 |
| Unit cell angles | 90.02, 90.02, 89.51 |
Refinement procedure
| Resolution | 45.190 - 2.500 |
| R-factor | 0.18707 |
| Rwork | 0.184 |
| R-free | 0.23615 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.754 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 115418 |
| <I/σ(I)> | 15.4 |
| Completeness [%] | 96.5 |
| Redundancy | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 293 | 0.2 M ammonium iodide, 20% PEG3350 |
