4W6K
Crystal Structure of Full-Length Split GFP Mutant D117C Disulfide Dimer, P 41 21 2 Space Group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-08-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0717 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 106.720, 106.720, 97.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 75.460 - 2.877 |
R-factor | 0.2536 |
Rwork | 0.249 |
R-free | 0.29410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b3p |
RMSD bond length | 0.003 |
RMSD bond angle | 0.854 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 75.460 |
High resolution limit [Å] | 2.870 |
Number of reflections | 13200 |
<I/σ(I)> | 22.07 |
Completeness [%] | 99.3 |
Redundancy | 12.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 0.5M KSCN, 0.1M NaAcetate pH 4.6 |