4W6H
Crystal Structure of Full-Length Split GFP Mutant D190C Disulfide Dimer, P 65 Space Group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-31 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0717 |
Spacegroup name | P 65 |
Unit cell lengths | 95.520, 95.520, 132.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 82.720 - 1.953 |
R-factor | 0.169 |
Rwork | 0.166 |
R-free | 0.19000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b3p |
RMSD bond length | 0.017 |
RMSD bond angle | 1.613 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: DEV_1555)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 82.720 |
High resolution limit [Å] | 1.953 |
Number of reflections | 49488 |
<I/σ(I)> | 16.42 |
Completeness [%] | 99.8 |
Redundancy | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 0.1M SPG Buffer pH8.0,25% PEG-1500 |