4W6G
Crystal Structure of Full-Length Split GFP Mutant D190C Disulfide Dimer, P 61 Space Group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-08-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9793 |
Spacegroup name | P 61 |
Unit cell lengths | 93.380, 93.380, 132.970 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 69.090 - 3.024 |
R-factor | 0.251 |
Rwork | 0.248 |
R-free | 0.27000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b3p |
RMSD bond length | 0.009 |
RMSD bond angle | 1.227 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: DEV_1555)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 69.090 |
High resolution limit [Å] | 3.024 |
Number of reflections | 12859 |
<I/σ(I)> | 16.73 |
Completeness [%] | 99.7 |
Redundancy | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | 20% 1,4-Butanediol, 0.1M Acetate pH 4.5 |