4W4Y

JNK2/3 in complex with 3-(4-{[(4-methylphenyl)carbamoyl]amino}-1H-pyrazol-1-yl)-N-(2-methylpyridin-4-yl)benzamide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL11-1
Synchrotron site	SSRL
Beamline	BL11-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-12-17
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.1270
Spacegroup name	P 21 21 21
Unit cell lengths	53.295, 71.573, 107.550
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.750 - 2.300
R-factor	0.1991
Rwork	0.196
R-free	0.25980
RMSD bond length	0.010
RMSD bond angle	1.160
Refinement software	BUSTER (2.11.5)

Data quality characteristics

	Overall
Low resolution limit [Å]	42.750
High resolution limit [Å]	2.300

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	EG 3350, ammonium tartrate