4V7Z
Structure of the Thermus thermophilus 70S ribosome complexed with telithromycin.
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Wavelength(s) | 0.979180 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 207.320, 437.990, 614.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.970 - 3.100 |
Rwork | 0.246 |
R-free | 0.28450 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.125 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.360 | 3.180 |
High resolution limit [Å] | 3.100 | 3.270 | 3.100 |
Rmerge | 0.182 | 0.673 | 1.146 |
Number of reflections | 914227 | ||
<I/σ(I)> | 8.16 | 1.97 | 0.99 |
Completeness [%] | 91.3 | 91.2 | 72.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |