4V7X
Structure of the Thermus thermophilus ribosome complexed with erythromycin.
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979490 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 210.470, 447.960, 620.170 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.610 - 3.000 |
Rwork | 0.243 |
R-free | 0.27790 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.250 | 3.080 |
High resolution limit [Å] | 3.000 | 3.160 | 3.000 |
Rmerge | 0.267 | 0.891 | 1.840 |
Number of reflections | 1153494 | ||
<I/σ(I)> | 8.08 | 1.79 | 0.89 |
Completeness [%] | 99.8 | 100 | 98.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |