4V3R
Designed armadillo repeat protein with 5 internal repeats, 2nd generation C-cap and 3rd generation N-cap.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Spacegroup name | I 4 |
Unit cell lengths | 129.910, 129.910, 70.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 91.860 - 1.950 |
R-factor | 0.17576 |
Rwork | 0.173 |
R-free | 0.22917 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4db6 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.719 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.880 | 2.060 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.090 | 0.480 |
Number of reflections | 41831 | |
<I/σ(I)> | 7.5 | 2 |
Completeness [%] | 98.1 | 98.2 |
Redundancy | 2.6 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M MAGNESIUM CHLORIDE 0.1 M TRISHCL, PH 8.5 30 % W/V PEG 4000 |