4UZV
Structure of a triple mutant of ASV-TfTrHb
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 78.367, 78.367, 89.806 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.400 |
R-factor | 0.30202 |
Rwork | 0.300 |
R-free | 0.34904 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bmm |
RMSD bond length | 0.014 |
RMSD bond angle | 1.175 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.520 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.130 | 0.320 |
Number of reflections | 4156 | |
<I/σ(I)> | 25 | 5.8 |
Completeness [%] | 99.8 | 99.7 |
Redundancy | 14.2 | 14.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |